What are the methods used to determine the boiling point of a compound?​

There are a variety of methods by which a sample's boiling point can be determined, including distillation, reflux, and by using a Thiele tube. The most straightforward method uses a Thiele tube, and has the advantage of using less than 0.5mL of material.

Distillation Method

There are simpler methods than a distillation to measure a compound's boiling point, and it is recommended to explore other options (e.g. Thiele tube) if this is the only goal. However, if materials are limited, or if a purification is planned anyhow, a distillation can be used to determine a compound's boiling point. The distillation technique is discussed in great detail in Chapter 5.

A simple distillation should suffice for most situations and at least 5mL of sample should be used in the distilling flask along with a few boiling stones or stir bar. As the bulk of the material distills, the highest temperature noted on the thermometer corresponds to the boiling point. A major source of error with this method is recording too low a temperature, before hot vapors fully immerse the thermometer bulb. 5 Be sure to monitor the thermometer periodically, especially when the distillation is active. Record the barometric pressure along with the boiling point.

Reflux Method

A reflux setup can also be used to determine a compound's boiling point. Reflux is when a liquid is actively boiling and condensing, with the condensed liquid returning to the original flask. It is analogous to a distillation setup, with the main difference being the vertical placement of the condenser.

Thiele Tube Method

There are a variety of methods by which a sample's boiling point can be determined, including distillation, reflux and by using a Thiele tube. The most straightforward method uses a Thilele tube, and has the advantage of using less than 0.5ml of material.

chemists can use the electron cloud model to assign electrons to different atomic orbitals. atomic orbitals also explain the patterns in the periodic table

explanation:

pure water does not conduct electricity very well. however, when certain substances are dissolved in water, the solution does conduct electricity. you can make a simple device that shows how well a solution conducts electricity. this device uses a flashlight bulb to indicate how well the solution conducts electricity. the better the solution conducts electricity, the brighter the bulb will glow.

explanation: