To prepare a sample in a capillary tube for a melting point determination, gently tap the tube into the sample with the
a) open,
b) closed end of the tube down.
Continue tapping until the sample
a) completely fills the tube
b) is a couple millimeters high,
c) has a single crystal in the tube.
Then, with the
a) closed,
b) open end of the tube down,
tap the sample down slowly or
a) heat the tube up,
b) drop the tube into a longer tube,
c) shake the tube in the air to move the sample down faster.
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